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. Author manuscript; available in PMC: 2019 Apr 20.
Published in final edited form as: Org Lett. 2018 Mar 27;20(8):2464–2467. doi: 10.1021/acs.orglett.8b00816

Scheme 4. Rh(III)-Catalyzed C–H Functionalization of Azoloaldimines 1 with Diazoketone 4a.

Scheme 4

aReactions performed on 0.3 mmol scale. bReaction performed with 4.0 equiv of PivOH at 120 °C.