Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C23H30O4 |
| M r | 370.47 |
| Crystal system, space group | Monoclinic, C c |
| Temperature (K) | 200 |
| a, b, c (Å) | 42.287 (9), 7.2848 (15), 6.7006 (13) |
| β (°) | 91.226 (12) |
| V (Å3) | 2063.7 (7) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.40 × 0.40 × 0.20 |
| Data collection | |
| Diffractometer | Bruker SMART X2S benchtop |
| Absorption correction | Multi-scan (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.64, 0.98 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 10387, 3095, 2363 |
| R int | 0.060 |
| (sin θ/λ)max (Å−1) | 0.602 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.044, 0.122, 1.05 |
| No. of reflections | 3095 |
| No. of parameters | 249 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.12, −0.18 |