| Nonius KappaCCD diffractometer | 8088 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.061 |
| Graphite monochromator | θmax = 25.0°, θmin = 1.4° |
| phi– and ω–scans | h = −14→13 |
| 33007 measured reflections | k = −29→29 |
| 10203 independent reflections | l = −22→22 |
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