Table 4. Hydrogen-bond geometry (Å, °) for complex 2 .
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| C1—H1⋯Cl1 | 0.96 (3) | 2.82 (3) | 3.252 (3) | 109 (2) |
| C3—H3A⋯Cl8i | 0.98 | 2.51 | 3.466 (4) | 164 |
| C3—H3B⋯Cl5i | 0.98 | 2.57 | 3.493 (4) | 158 |
| C6—H6A⋯O8ii | 0.98 | 2.59 | 3.431 (5) | 144 |
| C6—H6B⋯Cl9ii | 0.98 | 2.82 | 3.746 (4) | 158 |
| C7—H7A⋯Cl1A iii | 0.98 | 2.73 | 3.614 (6) | 150 |
| C7—H7B⋯Cl4iii | 0.98 | 2.60 | 3.518 (4) | 157 |
| C206—H206⋯Cl7iii | 0.94 | 2.79 | 3.719 (4) | 172 |
| C310—H310⋯Cl4ii | 0.94 | 2.83 | 3.714 (4) | 158 |
| C602—H602⋯Cl9ii | 0.94 | 2.62 | 3.557 (4) | 179 |
| C704—H704⋯Cl1iv | 0.94 | 2.82 | 3.534 (6) | 134 |
| C708—H708⋯Cl2 | 0.94 | 2.80 | 3.503 (4) | 132 |
| C710—H710⋯Cl5v | 0.94 | 2.72 | 3.614 (4) | 160 |
| C712—H712⋯Cl10iii | 0.94 | 2.81 | 3.734 (6) | 167 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
.