| Crystal data |
| Chemical formula |
C37H23N |
|
M
r
|
481.51 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
123 |
|
a, b, c (Å) |
9.2277 (2), 10.6445 (3), 14.639 (2) |
| α, β, γ (°) |
105.169 (2), 94.806 (2), 113.255 (2) |
|
V (Å3) |
1246.38 (18) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.07 |
| Crystal size (mm) |
0.12 × 0.12 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area-detector |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 2015 ▸) |
|
T
min, T
max
|
0.981, 0.995 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
22549, 5093, 4402 |
|
R
int
|
0.026 |
| (sin θ/λ)max (Å−1) |
0.625 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.035, 0.104, 1.04 |
| No. of reflections |
5093 |
| No. of parameters |
343 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.22, −0.19 |
