Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C6H10N3O+·C7H4ClO2 − |
| M r | 295.72 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 10.1148 (8), 11.2236 (8), 14.579 (1) |
| β (°) | 120.940 (5) |
| V (Å3) | 1419.57 (19) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.28 |
| Crystal size (mm) | 0.35 × 0.30 × 0.20 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.909, 0.946 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 10962, 3423, 2125 |
| R int | 0.024 |
| (sin θ/λ)max (Å−1) | 0.669 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.047, 0.152, 0.99 |
| No. of reflections | 3423 |
| No. of parameters | 188 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.26, −0.35 |