Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C32H26ClN3O2 |
| M r | 520.01 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c (Å) | 6.7722 (4), 11.5017 (8), 16.6305 (11) |
| α, β, γ (°) | 80.224 (3), 84.618 (3), 81.077 (3) |
| V (Å3) | 1258.09 (14) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.19 |
| Crystal size (mm) | 0.23 × 0.21 × 0.19 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.967, 0.974 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 25368, 4659, 3577 |
| R int | 0.035 |
| (sin θ/λ)max (Å−1) | 0.606 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.047, 0.133, 1.05 |
| No. of reflections | 4659 |
| No. of parameters | 347 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.37, −0.46 |