| Crystal data |
| Chemical formula |
C24H19Cl2N3O4
|
|
M
r
|
484.32 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
7.4028 (5), 7.4432 (5), 22.4616 (15) |
| α, β, γ (°) |
97.255 (5), 90.274 (5), 114.784 (5) |
|
V (Å3) |
1112.36 (14) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.33 |
| Crystal size (mm) |
0.61 × 0.26 × 0.04 |
| |
| Data collection |
| Diffractometer |
Stoe IPDS 2 |
| Absorption correction |
Integration (X-RED32; Stoe & Cie, 2002 ▸) |
|
T
min, T
max
|
0.901, 0.987 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
15409, 4604, 2261 |
|
R
int
|
0.083 |
| (sin θ/λ)max (Å−1) |
0.628 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.043, 0.089, 0.87 |
| No. of reflections |
4604 |
| No. of parameters |
298 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.13, −0.17 |
