Table 1. Data collection, model and map statistics.
| CypA | AP | WrpA | |
|---|---|---|---|
| Data-collection and Bragg statistics† | |||
| Space group | P212121 | P6322 | P4222 |
| Unit-cell parameters | |||
| a, b, c (Å) | 42.9, 52.4, 89.1 | 161.3, 161.3, 139.4 | 61.3, 61.3, 128.7 |
| α, β, γ (°) | 90.0, 90.0, 90.0 | 90.0, 90.0, 120.0 | 90.0, 90.0, 90.0 |
| Wavelength (Å) | 0.9795 | 0.9795 | 0.9787 |
| Oscillation range (°) | 0.5 | 0.15 | 1.0 |
| Data-collection temperature (K) | 273 | 100 | 100 |
| Beam divergence SD (°) | 0.0417 | 0.0285 | 0.0339 |
| Mosaicity (°) | 0.106 | 0.136 | 0.197 |
| Resolution range (Å) | 44.57–1.20 (1.24–1.20) | 49.36–2.00 (2.07–2.00) | 44.38–2.51 (2.60–2.51) |
| Multiplicity | 5.8 (4.8) | 6.3 (6.5) | 12.7 (12.7) |
| Completeness (%) | 93.6 (85.8) | 94.0 (92.7) | 99.6 (98.5) |
| 〈I/σ(I)〉 | 11.3 (3.9) | 26.2 (3.6) | 25.5 (4.6) |
| R merge | 0.113 (0.504) | 0.045 (0.348) | 0.061 (0.520) |
| R meas | 0.123 (0.564) | 0.049 (0.375) | 0.063 (0.542) |
| CC1/2 | 0.989 (0.872) | 1.000 (0.972) | 0.999 (0.962) |
| Wilson B (Å2) | 16.1 | 31.4 | 64.7 |
| Detector | PILATUS 6M | PILATUS 6M | MAR Mosaic 300 |
| SBGrid ID | 68 | 456 | 203 |
| Structure-refinement statistics | |||
| Resolution range (Å) | 44.57–1.20 | 49.36–2.00 | 44.37–2.50 |
| No. of non-H atoms | 1419 | 6731 | 1237 |
| Average B factor (Å2) | 21.4 | 46.2 | 77.0 |
| Solvent content (%) | 56 | 62 | 52 |
| R work/R free | 0.169/0.177 | 0.192/0.231 | 0.235/0.277 |
| Diffuse scattering statistics | |||
| Resolution range (Å) | 93.4–1.5 | 75.2–2.5 | 69.3–2.1 |
| CCFriedel pairs ‡ | 0.979 (0.623) | 0.954 (0.695) | 0.988 (0.689) |
| CCunsym, Friedel-sym ‡ § | 0.996 (0.915) | 0.994 (0.957) | 0.997 (0.930) |
| CCunsym, Laue-sym ‡ § | 0.993 (0.862) | 0.984 (0.887) | 0.994 (0.827) |
| Completeness (%) | 98.7 | 96.1 | 100.0 |
†
Values in parentheses are for the highest resolution shell.
‡
For values in parentheses, the average radial intensity was subtracted prior to applying symmetry operations.
§
Correlation coefficient between the unsymmetrized map and the map after applying the indicated symmetry operations.