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. 2018 Feb 13;74(Pt 3):349–351. doi: 10.1107/S2056989018002360
C1—C2 1.379 (2) C14—H14 0.9300
C1—C6 1.3873 (19) C15—C16 1.376 (2)
C1—H1 0.9300 C15—H15 0.9300
C2—C3 1.370 (2) C16—H16 0.9300
C2—H2 0.9300 C17—O2 1.1905 (16)
C3—C4 1.381 (2) C17—O3 1.3328 (18)
C3—H3 0.9300 C18—O3 1.4456 (19)
C4—C5 1.3942 (17) C18—H18A 0.9600
C4—H4 0.9300 C18—H18B 0.9600
C5—C6 1.3940 (19) C18—H18C 0.9600
C5—C10 1.4796 (18) C19—O4 1.1985 (15)
C6—C7 1.4777 (18) C19—O5 1.3256 (17)
C7—O1 1.2090 (17) C20—O5 1.4399 (19)
C7—C8 1.5397 (18) C20—H20A 0.9600
C8—C9 1.5212 (18) C20—H20B 0.9600
C8—C17 1.5392 (17) C20—H20C 0.9600
C8—C11 1.5408 (18) C21—C22 1.380 (2)
C9—C10 1.3457 (16) C21—C26 1.3867 (19)
C9—C19 1.4897 (18) C22—C23 1.384 (2)
C10—C21 1.4852 (18) C22—H22 0.9300
C11—C12 1.3844 (19) C23—C24 1.369 (3)
C11—C16 1.3866 (19) C23—H23 0.9300
C12—C13 1.3774 (19) C24—C25 1.365 (3)
C12—H12 0.9300 C24—H24 0.9300
C13—C14 1.371 (2) C25—C26 1.377 (3)
C13—H13 0.9300 C25—H25 0.9300
C14—C15 1.369 (2) C26—H26 0.9300
C2—C1—C6 120.04 (15) C14—C15—C16 120.74 (15)
C2—C1—H1 120.0 C14—C15—H15 119.6
C6—C1—H1 120.0 C16—C15—H15 119.6
C3—C2—C1 119.74 (14) C15—C16—C11 120.65 (15)
C3—C2—H2 120.1 C15—C16—H16 119.7
C1—C2—H2 120.1 C11—C16—H16 119.7
C2—C3—C4 120.68 (13) O2—C17—O3 124.69 (13)
C2—C3—H3 119.7 O2—C17—C8 126.72 (14)
C4—C3—H3 119.7 O3—C17—C8 108.57 (11)
C3—C4—C5 120.74 (14) O3—C18—H18A 109.5
C3—C4—H4 119.6 O3—C18—H18B 109.5
C5—C4—H4 119.6 H18A—C18—H18B 109.5
C6—C5—C4 117.90 (12) O3—C18—H18C 109.5
C6—C5—C10 120.27 (11) H18A—C18—H18C 109.5
C4—C5—C10 121.82 (12) H18B—C18—H18C 109.5
C1—C6—C5 120.89 (12) O4—C19—O5 123.97 (13)
C1—C6—C7 119.35 (13) O4—C19—C9 122.85 (13)
C5—C6—C7 119.76 (12) O5—C19—C9 113.11 (11)
O1—C7—C6 122.90 (12) O5—C20—H20A 109.5
O1—C7—C8 121.30 (11) O5—C20—H20B 109.5
C6—C7—C8 115.69 (11) H20A—C20—H20B 109.5
C9—C8—C17 110.48 (11) O5—C20—H20C 109.5
C9—C8—C7 110.63 (10) H20A—C20—H20C 109.5
C17—C8—C7 106.22 (10) H20B—C20—H20C 109.5
C9—C8—C11 112.92 (10) C22—C21—C26 118.68 (14)
C17—C8—C11 111.96 (10) C22—C21—C10 119.79 (12)
C7—C8—C11 104.24 (10) C26—C21—C10 121.49 (14)
C10—C9—C19 123.16 (12) C21—C22—C23 120.60 (17)
C10—C9—C8 122.34 (11) C21—C22—H22 119.7
C19—C9—C8 114.40 (10) C23—C22—H22 119.7
C9—C10—C5 119.96 (12) C24—C23—C22 120.1 (2)
C9—C10—C21 122.49 (12) C24—C23—H23 119.9
C5—C10—C21 117.40 (10) C22—C23—H23 119.9
C12—C11—C16 117.97 (13) C25—C24—C23 119.64 (18)
C12—C11—C8 122.16 (11) C25—C24—H24 120.2
C16—C11—C8 119.81 (12) C23—C24—H24 120.2
C13—C12—C11 120.92 (13) C24—C25—C26 120.94 (18)
C13—C12—H12 119.5 C24—C25—H25 119.5
C11—C12—H12 119.5 C26—C25—H25 119.5
C14—C13—C12 120.45 (14) C25—C26—C21 120.02 (18)
C14—C13—H13 119.8 C25—C26—H26 120.0
C12—C13—H13 119.8 C21—C26—H26 120.0
C15—C14—C13 119.25 (14) C17—O3—C18 115.77 (13)
C15—C14—H14 120.4 C19—O5—C20 117.16 (12)
C13—C14—H14 120.4
C6—C1—C2—C3 1.0 (2) C9—C8—C11—C16 176.27 (12)
C1—C2—C3—C4 −0.1 (2) C17—C8—C11—C16 −58.27 (16)
C2—C3—C4—C5 −0.8 (2) C7—C8—C11—C16 56.13 (14)
C3—C4—C5—C6 1.0 (2) C16—C11—C12—C13 −0.28 (18)
C3—C4—C5—C10 −179.82 (13) C8—C11—C12—C13 176.90 (12)
C2—C1—C6—C5 −0.8 (2) C11—C12—C13—C14 −0.3 (2)
C2—C1—C6—C7 179.38 (13) C12—C13—C14—C15 1.0 (2)
C4—C5—C6—C1 −0.2 (2) C13—C14—C15—C16 −1.0 (2)
C10—C5—C6—C1 −179.37 (12) C14—C15—C16—C11 0.4 (2)
C4—C5—C6—C7 179.65 (12) C12—C11—C16—C15 0.2 (2)
C10—C5—C6—C7 0.44 (18) C8—C11—C16—C15 −177.00 (13)
C1—C6—C7—O1 21.7 (2) C9—C8—C17—O2 138.57 (16)
C5—C6—C7—O1 −158.09 (14) C7—C8—C17—O2 −101.40 (17)
C1—C6—C7—C8 −154.54 (12) C11—C8—C17—O2 11.8 (2)
C5—C6—C7—C8 25.65 (18) C9—C8—C17—O3 −42.97 (14)
O1—C7—C8—C9 145.22 (13) C7—C8—C17—O3 77.06 (14)
C6—C7—C8—C9 −38.46 (15) C11—C8—C17—O3 −169.76 (11)
O1—C7—C8—C17 25.29 (17) C10—C9—C19—O4 140.82 (15)
C6—C7—C8—C17 −158.39 (11) C8—C9—C19—O4 −35.58 (19)
O1—C7—C8—C11 −93.12 (15) C10—C9—C19—O5 −42.04 (18)
C6—C7—C8—C11 83.21 (13) C8—C9—C19—O5 141.56 (12)
C17—C8—C9—C10 146.53 (12) C9—C10—C21—C22 −62.17 (19)
C7—C8—C9—C10 29.18 (17) C5—C10—C21—C22 113.49 (15)
C11—C8—C9—C10 −87.22 (15) C9—C10—C21—C26 120.02 (15)
C17—C8—C9—C19 −37.04 (15) C5—C10—C21—C26 −64.33 (17)
C7—C8—C9—C19 −154.38 (11) C26—C21—C22—C23 −0.2 (2)
C11—C8—C9—C19 89.22 (13) C10—C21—C22—C23 −178.11 (15)
C19—C9—C10—C5 179.15 (12) C21—C22—C23—C24 0.3 (3)
C8—C9—C10—C5 −4.73 (19) C22—C23—C24—C25 −0.6 (3)
C19—C9—C10—C21 −5.3 (2) C23—C24—C25—C26 0.9 (3)
C8—C9—C10—C21 170.82 (12) C24—C25—C26—C21 −0.9 (2)
C6—C5—C10—C9 −11.87 (19) C22—C21—C26—C25 0.6 (2)
C4—C5—C10—C9 168.95 (13) C10—C21—C26—C25 178.39 (13)
C6—C5—C10—C21 172.36 (12) O2—C17—O3—C18 −3.7 (2)
C4—C5—C10—C21 −6.82 (18) C8—C17—O3—C18 177.83 (14)
C9—C8—C11—C12 −0.86 (16) O4—C19—O5—C20 −4.2 (2)
C17—C8—C11—C12 124.60 (13) C9—C19—O5—C20 178.73 (14)
C7—C8—C11—C12 −121.00 (12)