Table 2. Experimental details.
| Crystal data | |
| Chemical formula | (C34H41N4Te)[HgI3(C4H8O2)] |
| M r | 1302.70 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 9.6074 (2), 25.4943 (6), 17.4326 (3) |
| β (°) | 95.152 (2) |
| V (Å3) | 4252.59 (15) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 6.51 |
| Crystal size (mm) | 0.27 × 0.21 × 0.13 |
| Data collection | |
| Diffractometer | Rigaku CCD dual source |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2015 ▸) |
| T min, T max | 0.238, 0.567 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 58708, 12625, 11288 |
| R int | 0.041 |
| (sin θ/λ)max (Å−1) | 0.728 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.080, 1.14 |
| No. of reflections | 12625 |
| No. of parameters | 448 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.45, −1.53 |