| Bruker SMART CCD area detector diffractometer | 2664 independent reflections |
| Radiation source: sealed tube | 1087 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.122 |
| phi and ω scans | θmax = 25.0°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −12→12 |
| Tmin = 0.785, Tmax = 0.856 | k = −9→9 |
| 17211 measured reflections | l = −24→23 |
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