Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C19H17N3O |
| M r | 303.22 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 10.5652 (7), 7.9136 (6), 20.8153 (13) |
| β (°) | 118.408 (4) |
| V (Å3) | 1530.77 (19) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.21 × 0.15 × 0.11 |
| Data collection | |
| Diffractometer | Bruker SMART CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2012 ▸) |
| T min, T max | 0.785, 0.856 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 17211, 2664, 1087 |
| R int | 0.122 |
| (sin θ/λ)max (Å−1) | 0.595 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.040, 0.092, 0.73 |
| No. of reflections | 2664 |
| No. of parameters | 212 |
| No. of restraints | 7 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.14, −0.15 |