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. 2018 Feb 28;74(Pt 3):419–421. doi: 10.1107/S2056989018003110
C1—C2 1.382 (2) C6—H6 0.9500
C1—C6 1.388 (2) C6'—C7' 1.376 (3)
C1—O1 1.428 (2) C6'—H6' 0.9500
C1'—C2' 1.379 (3) C7—C8 1.526 (3)
C1'—C7' 1.390 (3) C7—H7A 0.9800
C1'—S1 1.7486 (19) C7—H7B 0.9800
C2'—C3' 1.386 (3) C7—H7C 0.9800
C2'—H2' 0.9500 C7'—H7' 0.9500
C2—C3 1.400 (2) C8—C9 1.527 (3)
C2—C8 1.513 (2) C8—H8 1.0000
C3'—C4' 1.389 (3) C9—H9A 0.9800
C3'—H3' 0.9500 C9—H9B 0.9800
C3—C4 1.380 (3) C9—H9C 0.9800
C3—H3 0.9500 C10—O2 1.424 (3)
C4—O2 1.369 (2) C10—H10A 0.9800
C4—C5 1.403 (3) C10—H10B 0.9800
C4'—C6' 1.393 (3) C10—H10C 0.9800
C4'—C5' 1.504 (3) C11—H11A 0.9800
C5—C6 1.381 (3) C11—H11B 0.9800
C5—C11 1.503 (3) C11—H11C 0.9800
C5'—H5'1 0.9800 O1—S1 1.5967 (12)
C5'—H5'2 0.9800 O3—S1 1.4216 (14)
C5'—H5'3 0.9800 O4—S1 1.4221 (14)
C2—C1—C6 122.74 (16) C8—C7—H7B 109.5
C2—C1—O1 118.38 (15) H7A—C7—H7B 109.5
C6—C1—O1 118.64 (15) C8—C7—H7C 109.5
C2'—C1'—C7' 120.86 (18) H7A—C7—H7C 109.5
C2'—C1'—S1 120.13 (15) H7B—C7—H7C 109.5
C7'—C1'—S1 119.00 (14) C6'—C7'—C1' 119.26 (18)
C1'—C2'—C3' 118.97 (18) C6'—C7'—H7' 120.4
C1'—C2'—H2' 120.5 C1'—C7'—H7' 120.4
C3'—C2'—H2' 120.5 C2—C8—C7 111.27 (16)
C1—C2—C3 116.24 (16) C2—C8—C9 110.51 (17)
C1—C2—C8 123.71 (16) C7—C8—C9 110.87 (17)
C3—C2—C8 120.05 (16) C2—C8—H8 108.0
C2'—C3'—C4' 121.44 (18) C7—C8—H8 108.0
C2'—C3'—H3' 119.3 C9—C8—H8 108.0
C4'—C3'—H3' 119.3 C8—C9—H9A 109.5
C4—C3—C2 121.63 (17) C8—C9—H9B 109.5
C4—C3—H3 119.2 H9A—C9—H9B 109.5
C2—C3—H3 119.2 C8—C9—H9C 109.5
O2—C4—C3 123.76 (17) H9A—C9—H9C 109.5
O2—C4—C5 114.99 (16) H9B—C9—H9C 109.5
C3—C4—C5 121.26 (17) O2—C10—H10A 109.5
C3'—C4'—C6' 118.20 (18) O2—C10—H10B 109.5
C3'—C4'—C5' 121.55 (18) H10A—C10—H10B 109.5
C6'—C4'—C5' 120.25 (18) O2—C10—H10C 109.5
C6—C5—C4 117.33 (16) H10A—C10—H10C 109.5
C6—C5—C11 121.84 (18) H10B—C10—H10C 109.5
C4—C5—C11 120.83 (18) C5—C11—H11A 109.5
C4'—C5'—H5'1 109.5 C5—C11—H11B 109.5
C4'—C5'—H5'2 109.5 H11A—C11—H11B 109.5
H5'1—C5'—H5'2 109.5 C5—C11—H11C 109.5
C4'—C5'—H5'3 109.5 H11A—C11—H11C 109.5
H5'1—C5'—H5'3 109.5 H11B—C11—H11C 109.5
H5'2—C5'—H5'3 109.5 C1—O1—S1 120.71 (11)
C5—C6—C1 120.79 (17) C4—O2—C10 117.16 (15)
C5—C6—H6 119.6 O3—S1—O4 119.91 (9)
C1—C6—H6 119.6 O3—S1—O1 109.37 (8)
C7'—C6'—C4' 121.25 (18) O4—S1—O1 102.77 (8)
C7'—C6'—H6' 119.4 O3—S1—C1' 109.08 (9)
C4'—C6'—H6' 119.4 O4—S1—C1' 109.79 (9)
C8—C7—H7A 109.5 O1—S1—C1' 104.76 (8)