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. Author manuscript; available in PMC: 2018 May 16.
Published in final edited form as: Biochemistry. 2016 Aug 11;55(33):4654–4665. doi: 10.1021/acs.biochem.6b00472

Table 1.

X-ray data collection statistics

BshA/GlcNAc-mal BshA/GlcNAc-mal + UMP
Wavelength (Å) 1.07805 1.07813
Resolution limitsa (Å) 97.25 – 2.02 (2.13–2.02) 93.73–2.15 (2.27–2.15)
Number of independent reflections 46645 (6697) 40122 (5780)
Completeness (%) 99.9 (99.6) 100 (100)
Redundancy 7.4 (7.5) 9.6 (9.9)
Avg I/Avg σ(I) 19.5 (2.5) 15.0 (3.7)
Rmergeb (%) 5.7 (70.9) 9.3 (69.0)
a

Values in parentheses are for the highest resolution shell

b

Rmerge = Σ(|I – Ī|)/ ΣI X 100