Table 2.
Timed event | Oven program | |||||
---|---|---|---|---|---|---|
Event | Flow (mL·min−1) | Time (min) | Ramp | Rate (°C·min−1) | Temperature (°C) | Hold (min) |
Split | 0 | −0.51 | Initial | 0 | 45 | 1 |
Split | 50 | 1 | 1 | 20 | 200 | 0 |
Split | 20 | 5 | 2 | 4 | 320 | 5 |
Timed event | Oven program | |||||
---|---|---|---|---|---|---|
Event | Flow (mL·min−1) | Time (min) | Ramp | Rate (°C·min−1) | Temperature (°C) | Hold (min) |
Split | 0 | −0.51 | Initial | 0 | 45 | 1 |
Split | 50 | 1 | 1 | 20 | 200 | 0 |
Split | 20 | 5 | 2 | 4 | 320 | 5 |