Table 2. Experimental details.

Crystal data
Chemical formula	C8H8BrN3OS·C2H6OS
M r	352.26
Crystal system, space group	Triclinic, P
Temperature (K)	296
a, b, c (Å)	6.5411 (4), 7.3889 (6), 15.0662 (12)
α, β, γ (°)	78.772 (3), 86.872 (3), 87.376 (3)
V (Å3)	712.71 (9)
Z	2
Radiation type	Mo Kα
μ (mm−1)	3.17
Crystal size (mm)	0.30 × 0.20 × 0.20
Data collection
Diffractometer	Bruker Kappa APEXII CCD
Absorption correction	Multi-scan (SADABS; Bruker, 2004 ▸)
T min, T max	0.449, 0.569
No. of measured, independent and observed [I > 2σ(I)] reflections	6030, 3299, 2661
R int	0.018
(sin θ/λ)max (Å−1)	0.666
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.030, 0.106, 0.79
No. of reflections	3299
No. of parameters	165
H-atom treatment	H-atom parameters constrained
Δρmax, Δρmin (e Å−3)	0.27, −0.34

Computer programs: APEX2, SAINT and XPREP (Bruker, 2004 ▸), SIR92 (Altomare et al., 1993 ▸), SHELXL2017/1 (Sheldrick, 2015 ▸), PLATON (Spek 2009 ▸), Mercury (Macrae et al., 2008 ▸) and publCIF (Westrip, 2010 ▸).