| Crystal data |
| Chemical formula |
[Zn(C4H11N2)2(S2O3)2]·2H2O |
|
M
r
|
499.94 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.7631 (1), 10.5623 (2), 11.6072 (2) |
| α, β, γ (°) |
113.736 (1), 98.761 (1), 91.472 (1) |
|
V (Å3) |
967.49 (3) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.74 |
| Crystal size (mm) |
0.22 × 0.18 × 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEX CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2000 ▸) |
|
T
min, T
max
|
0.700, 0.768 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
19938, 7607, 5927 |
|
R
int
|
0.027 |
| (sin θ/λ)max (Å−1) |
0.782 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.032, 0.079, 1.01 |
| No. of reflections |
7607 |
| No. of parameters |
266 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.47, −0.36 |
