Figure 8.
Synthesis of aerobactin precursor (3S,2′S)-citryl-ahLys. Reaction conditions: (a) Pd/C, H2, EtOH, room temperature, 1 h; (b) SOCl2, 85 °C, 1 h; (c) Et3N, 0 °C to room temperature, 2 h; (d) LiOH, THF:H2O.
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