Table 1.
Data collection and refinement statistics.
| Data collection | LC/HA |
|---|---|
| Wavelength (Å) | 0.97918 |
| Resolution (Å) | 109.55–2.09 (2.13–2.09) |
| Space group | C 2 2 21 |
| Cell dimensions | |
| a, b, c (Å) | 76.2, 160.7, 219.1 |
| α, β, γ (°) | 90, 90, 90 |
| Completeness (%) | 96.0 (96.7) |
| Redundancy | 3.3 (3.3) |
| R merge (%) | 10.0 (39.3) |
| Mean I/σ(I) | 8.2 (2.0) |
| Refinement | |
| Resolution (Å) | 54.05–2.09 |
| No. reflections | 76 565 |
| R work/Rfree (%) | 17.61/19.12 |
| No. atoms | |
| Protein | 6924 |
| Ligand/ion | 19 |
| Water | 584 |
| B-factors (Å2) | |
| Protein | 36.2 |
| Ligand/ion | 42.9 |
| Water | 41.9 |
| r.m.s. deviations | |
| Bond lengths (Å) | 0.013 |
| Bond angles (°) | 1.24 |
Values in parentheses are for the highest resolution shell.