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Course of ZnO NPs syntheses in the MSS2 reactor.
| Sample Name | 1st Stage—Pre-Heating Duration, 0→4 bar, (min:s) | 2nd Stage—Heating Duration, 4 bar, ~230 °C, (min:s) | 3rd Stage—Cooling down Duration, ~230 °C→~90 °C | Total Synthesis Duration (min:s) |
|---|---|---|---|---|
| ZnO-1 kW | 6:47 | 12:00 | a few seconds | ~18:47 |
| ZnO-2 kW | 2:57 | 12:00 | a few seconds | ~14:57 |
| ZnO-3 kW | 1:48 | 12:00 | a few seconds | ~13:48 |
