Table 2.
13C (100 MHz) NMR data of compounds 1, 2, and 4–6 (in CD3OD).
| No. | 1 | 2 | 4 | 5 | 6 | 
|---|---|---|---|---|---|
| 1 | 204.6, C | 203.0, C | 162.1, C | 204.4, C | 204.4, C | 
| 2 | 36.1, CH2 | 34.5, CH2 | 36.1, CH2 | 36.1, CH2 | |
| 3 | 32.7, CH2 | 31.4, CH2 | 156.3, C | 32.7, CH2 | 32.8, CH2 | 
| 4 | 68.6, CH | 67.2, CH | 98.9, CH | 68.6, CH | 68.7, CH | 
| 4a | 150.2, C | 147.7, C | 135.3, C | 151.3, C | 151.2, C | 
| 5 | 102.2, CH | 100.4, CH | 135.8, C | 101.9, CH | 101.8, CH | 
| 6 | 164.8, C | 164.1, C | 158.5, C | 166.2, C | 166.1, C | 
| 7 | 119.1, C | 111.9, C | 100.2, CH | 116.7, C | 116.7, C | 
| 8 | 162.7, C | 162.0, C | 161.0, C | 164.3, C | 164.3, C | 
| 8a | 111.1, C | 109.6, C | 101.2, C | 110.8, C | 110.8, C | 
| 9 | 56.4, CH3 | 55.0, CH3 | 19.5, CH3 | 56.3, CH3 | 56.2, CH3 | 
| 10 | 63.4, CH | 25.3, CH2 | 56.4, CH3 | 70.3, CH | 70.4, CH | 
| 11 | 22.2, CH3 | 60.1, CH2 | 61.6, CH3 | 20.0, CH3 | 20.1, CH3 | 
| 1′ | 204.2, C | 204.2, C | |||
| 2′ | 36.1, CH2 | 36.1, CH2 | |||
| 3’ | 32.7, CH2 | 32.8, CH2 | |||
| 4′ | 68.6, CH | 68.6, CH | |||
| 4a′ | 150.3, C | 150.3, C | |||
| 5′ | 101.3, CH | 101.3, CH | |||
| 6′ | 165.9, C | 165.9, C | |||
| 7′ | 113.0, C | 113.1, C | |||
| 8′ | 163.7, C | 163.6, C | |||
| 8a′ | 110.7, C | 110.7, C | |||
| 9′ | 56.2, CH3 | 56.1, CH3 | |||
| 10′ | 59.6, CH2 | 59.8, CH2 |