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. 2018 May 29;9:989. doi: 10.3389/fmicb.2018.00989

Table 1.

Quantitative analysis of the exudates of Lyophyllum sp. strain Karsten and Trichoderma asperellum 302 for the identification of oxalic acid, using high-performance liquid chromatography (HPLC). Oxalic acid was used as an external standard and M9 medium as a negative control.

Compounds Retention time (min) Area Height Concentration % (w/v)
MilliQ 0.00 0 0 0.000
Oxalic acid_0.01% 2.48 386,101 27,450 0.010
Oxalic acid_0.01% 2.48 369,726 27,375 0.010
Oxalic acid_0.05% 2.39 5,071,290 562,392 0.051
Oxalic acid_0.05% 2.39 5,033,482 567,899 0.051
Oxalic acid_0.10% 2.39 9,400,274 1,084,105 0.099
Oxalic acid_0.10% 2.38 9,960,133 1,074,788 0.102
M9 medium 2.37 86,273 12,120 0.001
M9 medium 2.37 103,940 14,645 0.001
M9+0.1% Oxalic acid 2.37 8,007,944 1,290,413 0.092
M9+0.1% Oxalic acid 2.38 8,026,472 1,301,304 0.092
Lyophyllum sp. strain Karsten 2.41 7,795,023 719,831 0.090
Lyophyllum sp. strain Karsten 2.41 6,417,830 710,125 0.074
Lyophyllum sp. strain Karsten 1:5 2.36 3,554,342 518,881 0.041
Lyophyllum sp. strain Karsten 1:5 2.36 3,243,405 494,120 0.037
Lyophyllum sp. strain Karsten 1:10 2.36 2,205,528 388,395 0.025
Lyophyllum sp. strain Karsten 1:10 2.35 2,217,147 359,645 0.025
T. asperellum 302 2.40 8,137,144 683,484 0.093
T. asperellum 302 2.40 7,592,703 680,421 0.087
T. asperellum 302 1:5 2.36 1,576,896 286,151 0.018
T. asperellum 302 1:5 2.35 1,500,720 262,248 0.017
T. asperellum 302 1:10 2.36 847,009 162,324 0.010
T. asperellum 302 1:10 2.35 848,337 162,203 0.010