Table 1.
Glycosylsphingosine | Ganglioside Product |
C18 cartridge elution condition |
Yield (%) |
---|---|---|---|
GM3βSph (6) | GM3 (1) | 80% CH3CN in H2O | 99 |
GM2βSph (7) | GM2 (12) | 50% CH3CN in H2O | 98 |
GM1βSph (8) | GM1 (13) | 50% CH3CN in H2O | 99 |
Fuc-GM1βSph (9) | Fucosyl GM1 (2) | 50% CH3CN in H2O | 99 |
GD3βSph (10) | GD3 (3) | 50% CH3CN in H2O | 99 |
GD2βSph (11) | GD2 (4) | 40% CH3CN in H2O | 98 |