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Series of hyperpolarized single‐scan 13C NMR spectra of 5–5d (100 mM) and [IrCl(COD)(IMes)] (5 mM) in methanol‐d 4 under p‐H2 after transfer at 0.5 G. Thermally polarized reference 13C NMR spectrum (top), acquired over 4,096 scans. ε = enhancement factor, fold gain
