Table 6. Evaluation of the stability of DAS in rat plasma.
Stability | Concentration added (ng/mL) | Mean recovery (%) ±RSDa |
---|---|---|
Auto-sampler stability (10°C, 56 h) | 3 | 97.30±5.41 |
450 | 98.47±3.14 | |
Short-term stability (25°C, 6 h) | 3 | 96.13±2.85 |
450 | 97.24±3.83 | |
Long-term stability (-30°C, 30 days) | 3 | 97.93±2.58 |
450 | 97.26±0.81 | |
Freeze-thaw stability (-30°C, 3 cycles) | 3 | 101.43±1.22 |
450 | 99.47±0.24 | |
Refrigerator (4°C, 3 months) | 3 | 99.89±1.76 |
450 | 98.09±3.93 |
aMean recovery (%) ± RSD of six determinations.