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. 2016 Mar 19;11(1):13–17. doi: 10.1016/j.joto.2016.03.001

Table 1.

The total arsenic measurement methods used by several authors.

Authors Sample Method Preparation method
Valentine et al., 1979 Blood and hair HGAAS Wet ash with nitric/perchloric acids; reduction with sodium borohydride
Foa et al., 1984 Blood HGAAS Wet ash with nitric/perchloric acids; reduction with sodium borohydride
Curatola et al., 1978 Hair HGAAS Wet ashing with nitric/sulfuric acids and hydrogen peroxide; reduction to arsine with sodium borohydride
Agahian et al., 1990 Nails HGAAS Wet ashing with nitric/sulfuric acids and hydrogen peroxide; reduction to arsine with sodium borohydride
Mushak et al., 1977 Soft tissue GFAAS Digestion with nitric/sulfuric acids; complexation with DDDC in potassium iodide; extraction with chloroform
Pinto et al., 1976 Urine Colorimetric photometry Digestion with nitric and perchloric acid; reduction with tin chloride; generation arsine by addition of zinc; reaction with SDDC
Landsberger and Simsons, 1987 Urine NAA Irradiate epithermally