| Crystal data |
| Chemical formula |
C24H18O4·2C3H7NO |
|
M
r
|
516.57 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
294 |
|
a, b, c (Å) |
6.0569 (5), 9.5801 (5), 11.9941 (8) |
| α, β, γ (°) |
72.867 (2), 84.649 (2), 86.710 (2) |
|
V (Å3) |
661.86 (8) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.09 |
| Crystal size (mm) |
0.25 × 0.24 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII DUO CCD area-detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.961, 0.991 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
21963, 3039, 1944 |
|
R
int
|
0.043 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.057, 0.177, 1.07 |
| No. of reflections |
3039 |
| No. of parameters |
178 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.17, −0.19 |
