STOE IPDS2T diffractometer | 3344 independent reflections |
Radiation source: fine-focus sealed tube | 2636 reflections with I > 2σ(I) |
Detector resolution: 6.67 pixels mm-1 | Rint = 0.034 |
ω scans | θmax = 29.2°, θmin = 3.2° |
Absorption correction: numerical face indexed | h = −14→11 |
Tmin = 0.771, Tmax = 0.942 | k = −12→12 |
13324 measured reflections | l = −18→18 |