Table 2. Experimental details.
| Crystal data | |
| Chemical formula | (C34H41N4Se)2[Hg(CNSe)4] |
| M r | 1789.84 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 12.7788 (15), 27.276 (3), 20.180 (3) |
| β (°) | 95.591 (2) |
| V (Å3) | 7000.4 (15) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 5.37 |
| Crystal size (mm) | 0.24 × 0.23 × 0.19 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2002 ▸) |
| T min, T max | 0.267, 0.336 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 46553, 9030, 8196 |
| R int | 0.095 |
| (sin θ/λ)max (Å−1) | 0.676 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.040, 0.097, 1.03 |
| No. of reflections | 9030 |
| No. of parameters | 463 |
| No. of restraints | 147 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.97, −2.10 |