| Crystal data |
| Chemical formula |
C17H15N3O2·CH4O |
|
M
r
|
325.36 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
173 |
|
a, b, c (Å) |
7.1597 (11), 9.8762 (16), 12.243 (2) |
| α, β, γ (°) |
110.426 (3), 94.051 (3), 93.378 (3) |
|
V (Å3) |
806.0 (2) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.09 |
| Crystal size (mm) |
0.14 × 0.13 × 0.12 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2005 ▸) |
|
T
min, T
max
|
0.987, 0.989 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4168, 2830, 2071 |
|
R
int
|
0.025 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.109, 1.03 |
| No. of reflections |
2830 |
| No. of parameters |
222 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.21, −0.23 |
