Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C10H5BrF6O |
| M r | 335.04 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 153 |
| a, b, c (Å) | 14.156 (5), 5.0111 (16), 15.535 (5) |
| β (°) | 104.316 (5) |
| V (Å3) | 1067.7 (6) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 3.92 |
| Crystal size (mm) | 0.23 × 0.09 × 0.06 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII DUO |
| Absorption correction | Multi-scan (SADABS; Bruker, 2012 ▸) |
| T min, T max | 0.442, 0.759 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 11628, 2405, 1741 |
| R int | 0.060 |
| (sin θ/λ)max (Å−1) | 0.646 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.103, 1.03 |
| No. of reflections | 2405 |
| No. of parameters | 163 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.78, −1.12 |