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. Author manuscript; available in PMC: 2018 Jun 15.
Published in final edited form as: Biomed Chromatogr. 2017 Oct 17;32(3):10.1002/bmc.4102. doi: 10.1002/bmc.4102

TABLE 3.

Unstable eicosanoids in different matrices under various storage conditionsa

Storage condition Autosampler at 4 °C Freeze-thaw three cycles at −20°C Bench-top at room temperature Long-term stability at −20°C Long-term stability at −80°C
Matrix Extracted matrix Original matrix Original matrix Extracted matrix Original matrix Extracted matrix Original matrix
Time Up to 24 h Up to 3 cycles Up to 2 h Up to 8 h Up to 4h Up to 180 days Up to 3 days Up to 7 days Up to 180 days
Stock solution 8 and 27 17 and 42 All stable 16 and 41 NA 16 and 41 NA NA 16 and 41
Serum 8 and 27 3, 15, 16, 18, 33, 36, 41, 42, 43 and 44 3, 15, 16, 41 and 42 3,15, 16, 18, 22, 33, 39, 41, 42, 43, 27 and 44 All stable 15,16, 18, 22, 33, 36, 38, 41, 42, 43 and 44 15, 16 1, 14, 15, 16, 33, 34 and 41 NA
a

Analytes with >20% loss by the reported time intervals under different storage conditions are presented.