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aReaction conditions: 1 (0.2 mmol) in 1.2 mL solvent, 1/[Rh(COD)Cl]2/L1 ratio = 100/0.5/1; yield was determined with isolated THIQ products; ee was determined by GC or HPLC with a chiral stationary phase; eperformed in dioxane/i-PrOH = 2 : 1 (v/v) at 60 °C under 60 atm H2 with 2% catalyst.
