Table 2. Experimental parameters of electron diffraction dataset for structure solution of Zr-CAU-30-as in space group I41/acd.
Tilt range (°) | –65/+58 |
No. of total reflections | 18 149 |
No. of independent reflections | 2021 |
Reflection coverage (%) | 99 |
Resolution (Å) | 1.0 |
R int | 0.344 |
Overall U (Å2) | 0.023 |
Residual R (SIR2014) | 0.173 |