Table 2. Experimental parameters of electron diffraction dataset for structure solution of Zr-CAU-30-as in space group I41/acd.
| Tilt range (°) | –65/+58 |
| No. of total reflections | 18 149 |
| No. of independent reflections | 2021 |
| Reflection coverage (%) | 99 |
| Resolution (Å) | 1.0 |
| R int | 0.344 |
| Overall U (Å2) | 0.023 |
| Residual R (SIR2014) | 0.173 |