Table 2.

Crystallographic data for compound 2c.

Entry	Data
formula	C10H9FN2O3
Mr	224.19
crystal size, mm3	0.032 × 0.162 × 0.247
crystal system	orthorhombic
space group	Pna21
cell constants
a, Å	10.0315(3)
b, Å	15.4164(5)
c, Å	6.5161(2)
V, Å3	1007.71(5)
Z	4
Dx, Mg m−3	1.48
μ, mm−1	1.06
F(000), e	464
T, K	100(2)
λ, Å	1.54178
2θmax, deg	137
transmissions	0.78–0.97
refl. meas./indep./Rint	10003/1813/0.034
ref. parameters	182
restraints	118
R [F ≥ 4 σ(F)]	0.032
wR (F2, all refl.)	0.086
S	1.05
Δρmax, e Å−3	0.145/−0.194