Table 1.
Analytical data of derivatives EMAC 3039–3064.
| C–H–N |
|||||||
|---|---|---|---|---|---|---|---|
| Compound | M.w. | Yield % | M.p. °C. | Crystals color | Cryst. solvent | Calc. | Found |
| EMAC 3039 | 449.75 | 71.15 | >250d | Orange | Water/ethanol | C, 58.61; H, 3.55; N, 15.19 | C, 58.57; H, 3.53; N, 15.17 |
| EMAC 3040 | 433.29 | 84.25 | 210–212 | Orange | Water/ethanol | C, 61.35; H, 3.72; N, 15.90 | C, 61.45; H, 3.70; N, 15.87 |
| EMAC 3041 | 494.20 | 91.70 | >250d | Orange | Water/ethanol | C, 52.31; H, 3.17; N, 13.56 | C, 52.33; H, 3.15; N, 13.53 |
| EMAC 3042 | 460.30 | 76.05 | >250d | Orange | Water/ethanol | C, 56.98; H, 3.45; N, 18.46 | C, 56.95; H, 3.41; N, 18.43 |
| EMAC 3043 | 491.40 | 82.40 | >250d | Orange | Water/ethanol | C, 70.22; H, 4.42; N, 13.65 | C, 70.27; H, 4.43; N, 13.62 |
| EMAC 3044 | 440.31 | 81.75 | >250d | Orange | Water/ethanol | C, 63.49; H, 3.65; N, 19.49 | C, 63.51; H, 3.62; N, 19.44 |
| EMAC 3045 | 406.84 | 73.75 | >250d | Orange | Water/ethanol | C, 58.37; H, 3.27; N, 15.13 | C, 58.38; H, 3.23; N, 15.11 |
| EMAC 3046 | 460.30 | 79.30 | >250d | Orange | Water/ethanol | C, 56.98; H, 3.45; N, 18.46 | C, 57.02; H, 3.44; N, 18.44 |
| EMAC 3047 | 484.19 | 84.65 | >250d | Yellow | Water/ethanol | C, 53.61; H, 3.00; N, 13.89 | C, 53.60; H, 2.98; N, 13.87 |
| EMAC 3048 | 429.33 | 59.40 | >250d | Light orange | Water/ethanol | C, 65.50; H, 4.63; N, 16.08 | C, 65.48; H, 4.61; N, 16.06 |
| EMAC 3049 | 445.33 | 83.00 | >250d | Orange | Water/ethanol | C, 62.62; H, 4.43; N, 15.37 | C, 62.61; H, 4.45; N, 15.33 |
| EMAC 3050 | 415.30 | 61.40 | >250d | Ocher yellow | Water/ethanol | C, 64.65; H, 4.22; N, 16.75 | C, 64.63; H, 4.23; N, 16.68 |
| EMAC 3051 | 439.75 | 69.35 | >250d | Yellow | Water/ethanol | C, 53.61; H, 3.00; N, 13.89 | C, 53.58; H, 3.01; N, 13.85 |
| EMAC 3052 | 484.19 | 59.56 | >250d | Orange | Water/ethanol | C, 53.61; H, 3.00; N, 13.89 | C, 53.61; H, 2.99; N, 13.88 |
| EMAC 3053 | 467.74 | 57.70 | >250d | Orange-yellow | Water/ethanol | C, 55.89; H, 3.13; N, 14.48 | C, 55.88; H, 3.14; N, 14.44 |
| EMAC 3054 | 528.65 | 70.00 | >250d | Orange | Water/ethanol | C, 48.29; H, 2.70; N, 12.51 | C, 48.31; H, 2.67; N, 12.48 |
| EMAC 3055 | 494.75 | 66.70 | >250d | Orange | Water/ethanol | C, 52.24; H, 2.92; N, 16.92 | C, 52.20; H, 2.94; N, 16.89 |
| EMAC 3056 | 525.85 | 58.95 | >250d | Orange | Water/ethanol | C, 64.79; H, 3.85; N, 12.59 | C, 64.76; H, 3.84; N, 12.57 |
| EMAC 3057 | 474.76 | 53.70 | >250d | Orange-yellow | Water/ethanol | C, 57.94; H, 3.07; N, 17.78 | C, 58.02; H, 3.05; N, 17.77 |
| EMAC 3058 | 441.28 | 27.20 | >250d | Yellow | Water/ethanol | C, 53.40; H, 2.74; N, 13.84 | C, 53.38; H, 2.76; N, 13.80 |
| EMAC 3059 | 494.65 | 57.60 | >250° | Orange | Water/ethanol | C, 52.24; H, 2.92; N, 16.92 | C, 52.21; H, 2.94; N, 16.88 |
| EMAC 3060 | 518.54 | 29.89 | >250° | Red | Water/ethanol | C, 49.39; H, 2.53; N, 12.80 | C, 49.37; H, 2.50; N, 12.74 |
| EMAC 3061 | 463.68 | 59.10 | >250° | Orange-red | Water/ethanol | C, 59.60; H, 3.95; N, 14.63 | C, 59.58; H, 3.97; N, 14.60 |
| EMAC 3062 | 479.68 | 51.00 | >250° | Red | Water/ethanol | C, 57.21; H, 3.79; N, 14.05 | C, 57.18; H, 3.81; N, 14.00 |
| EMAC 3063 | 449.65 | 55.60 | >250° | Orange | Water/ethanol | C, 58.61; H, 3.55; N, 15.19 | C, 58.56; H, 3.54; N, 15.16 |