Table 1.

Crystallographic Data Collection and Refinement Statistics

	PDB entry 3LWW
Data Collection
wavelength (Å)	0.918
space group	P1211
unit cell dimensions (Å)	a = 101.65, b = 101.73, c = 101.96
unit cell angles (deg)	α = γ = 90, β = 110.88
resolution range (Å)	15–3.15
B value from Wilson plot (Å2)	73.90
total no. of observations	63234
no. of unique observations	32721
completeness (%)	99.2 (69.0)a
Rsymb (%)	12.5 (53.5)a
〈I〉/〈σ(I)〉	16.3 (1.2)a
Refinement
no. of reflections (15–3.15 Å)	59672
Rwork/Rfreec (%)	26.35/31.29
no. of water molecules	0
B value of model (Å2)	88.17
rmsdd from ideal bond lengths (Å)	0.003
rmsdd from ideal bond angles (deg)	0.716
Ramachandran plot (%) (residues)
core region	82.7 (1365)
allowed region	15.9 (262)
generously allowed region	1.1 (18)
disallowed region	0.3 (5)

^aThe numbers in parentheses refer to the statistics for the outer resolution shell (3.26–3.15 Å).

^bR_sym = Σ_i,h|I(i,h) − 〈I(h)〉|/Σ_i,h|I(i,h)|, where I(i,h) and 〈I(h)〉 are the ith and mean measurements of intensity of reflection h, respectively.

^cThe R_free value was calculated using 5% of the data.

^dRoot-mean-square deviation.