Table 2. Summary of chemical shifts of selected proton resonances of 4b before and after addition of one molar equivalent of TBAH2PO4 in CDCl3.
aThe solution of 4b was prepared from diffraction grade single crystals of 4b, which contained two DMF molecules of crystallization per equivalent of receptor.
bObtained by treating with the TBA+ salt of H2PO4–; see text for details.