Table 2. Scope of the C-5 selective iodination protocol a .
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a<5% bis-iodination was observed in all cases. NIS = N-iodosuccinimide. [a] 5 mol% [RhCp*Cl2]2 and 27 mol% AgNTf2 were used. [b] Run at 65 °C and 75 W.
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a<5% bis-iodination was observed in all cases. NIS = N-iodosuccinimide. [a] 5 mol% [RhCp*Cl2]2 and 27 mol% AgNTf2 were used. [b] Run at 65 °C and 75 W.