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. 2018 Jun 22;9:2437. doi: 10.1038/s41467-018-04862-w

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© The Author(s) 2018

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 5 — Evolution of LiNi_0.6Mn_0.2Co_0.2O₂ charged to 4.7 V during heating. a In situ X-ray diffraction (XRD) measurements. b–d Direct high angle annular dark field (HAADF) observation of the inner bulk degradation at gradually increased magnifications, enabled by focus ion beam (FIB) milled cross-section sample. The yellow square region in (b) is enlarged as (c) and the yellow square region in (c) is enlarged as (d). The scale bars are 200 nm in (b), 50 nm in (c), and 2 nm in (d)