Table 2.
No. | 1 a | 2 a | 3 a | 4 b | 5 b | 6 a | 7 a |
---|---|---|---|---|---|---|---|
1 | 84.0, CH | 84.5, CH | 77.2, CH | 68.8, CH | 69.3, CH | 72.6, CH | 155.1, CH |
2 | 37.3, CH2 | 37.9, CH2 | 36.2, CH2 | 39.8, CH2 | 39.9, CH2 | 36.3, CH2 | 125.1, CH |
3 | 173.6, C | 176.7, C | 173.2, C | 171.2, C | 171.0, C | 172.9, C | 203.2, C |
4 | 79.7, C | 79.6, C | 144.4, C | 84.8, C | 84.1, C | 86.7, C | 45.1, C |
5 | 61.4, CH | 61.5, CH | 51.3, CH | 50.2, CH | 49.5, CH | 51.3, CH | 53.0, CH |
6 | 68.3, CH | 68.3, CH | 73.4, CH | 23.3, CH2 | 72.6, CH | 72.7, CH | 68.8, CH |
7 | 45.3, CH2 | 45.3, CH2 | 43.3, CH2 | 40.6, CH2 | 43.3, CH2 | 43.3, CH2 | 43.4, CH2 |
8 | 81.5, C | 81.6, C | 81.2, C | 80.9, C | 79.9, C | 80.4, C | 79.3, C |
9 | 48.1, CH | 48.1, CH | 44.2, CH | 44.8, CH | 44.4, CH | 45.1, CH | 46.9, CH |
10 | 46.5, C | 46.4, C | 45.6, C | 45.3, C | 45.4, C | 45.1, C | 39.4, C |
11 | 19.4, CH2 | 19.4, CH2 | 19.7, CH2 | 17.5, CH2 | 17.2, CH2 | 17.6, CH2 | 16.9, CH2 |
12 | 98.5, C | 98.6, C | 99.0, C | 98.2, C | 98.3, C | 98.3, C | 97.3, C |
13 | 167.1, C | 167.2, C | 167.1, C | 164.5, C | 164.5, C | 164.6, C | 164.8, C |
14 | 162.2, C | 162.2, C | 162.2, C | 160.8, C | 161.0, C | 162.3, C | 160.5, C |
15 | 102.2, CH | 102.0, CH | 101.8, CH | 100.6, CH | 100.6, CH | 101.7, CH | 100.3, CH |
16 | 165.1, C | 165.2, C | 164.8, C | 163.3, C | 162.8, C | 166.8, C | 162.7, C |
17 | 19.5, CH3 | 19.5, CH3 | 19.5, CH3 | 19.5, CH3 | 19.5, CH3 | 19.5, CH3 | 19.7, CH3 |
18 | 23.0, CH3 | 23.0, CH3 | 22.1, CH3 | 20.9, CH3 | 21.9, CH3 | 22.0, CH3 | 22.0, CH3 |
19 | 12.4, CH3 | 12.5, CH3 | 15.3, CH3 | 15.2, CH3 | 16.2, CH3 | 16.0, CH3 | 18.1, CH3 |
20 | 30.5, CH3 | 30.6, CH3 | 117.7, CH2 | 34.9, CH3 | 33.9, CH3 | 33.9, CH3 | 26.6, CH3 |
21 | 25.5, CH3 | 25.6, CH3 | 26.5, CH3 | 24.0, CH3 | 26.4, CH3 | 26.2, CH3 | 22.8, CH3 |
22 | 171.6, C | 171.7, C | 171.5, C | 170.2, C | 171.2, C | 169.7, C | |
23 | 21.3, CH3 | 21.3, CH3 | 20.9, CH3 | 21.4, CH3 | 21.3, CH3 | 21.5, CH3 | |
24 | 52.3, OCH3 | 172.2, C | 171.1, C | ||||
25 | 21.4, CH3 | 20.6, CH3 |
a Recorded at 100 MHz in methanol-d4; b recorded at 150 MHz in acetone-d6.