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Molecular structure of 3 from single-crystal X-ray diffraction with anisotropic displacement parameters drawn at the 50% probability level. Hydrogen atoms and cocrystallized 1 and 2 are omitted for clarity. Selected bond lengths (Å) and angles (deg): Re1–N3 1.861(8), Re1–N1 1.937(7), N3–N4 1.202(10), Re2–N4 1.886(8), Re2–N4 1.949(8), N1–Re1–Cl2 146.30(2), P1–Re1–P2 157.38(9), P3–Re2–P4 156.28(9), N2–Re2–Cl2 146.6(3), Cl1–Re1–Re2–Cl2 112.0(6).
