Table 4.
13C NMR spectroscopic data of compounds 5–7
| No. | 5*a | 6*a | 7*a |
|---|---|---|---|
| 1 | 162.2 | 162.2 | 161.9 |
| 2 | 117.4 | 117.5 | 117.5 |
| 3 | 146.7 | 146.8 | 147.7 |
| 4 | 121.9 | 121.9 | 121.2 |
| 5 | 113.0 | 110.9 | 113.3 |
| 6 | 166.1 | 165.4 | 164.1 |
| 7 | 108.1 | 107.8 | 106.3 |
| 8 | 162.0 | 161.8 | 161.7 |
| 9 | 188.4 | 188.6 | 188.6 |
| 10 | 57.3 | 57.6 | 57.3 |
| 1a | 117.7 | 118.2 | 118.5 |
| 4a | 139.8 | 140.6 | 141.9 |
| 5a | 144.5 | 145.5 | 144.1 |
| 8a | 116.5 | 117.8 | 116.1 |
| 3-Me | 21.8 | 22.0 | 22.2 |
| 1′ | 162.9 | 162.9 | 162.0 |
| 2′ | 117.5 | 117.7 | 117.6 |
| 3′ | 147.5 | 147.6 | 147.7 |
| 4′ | 121.4 | 121.6 | 121.2 |
| 5′ | 111.7 | 112.6 | 111.0 |
| 6′ | 164.9 | 165.2 | 164.9 |
| 7′ | 104.2 | 106.2 | 105.5 |
| 8′ | 162.0 | 162.0 | 161.4 |
| 9′ | 188.4 | 188.3 | 188.5 |
| 10′ | 57.5 | 57.5 | 57.4 |
| 1a′ | 117.9 | 117.2 | 118.6 |
| 4a′ | 142.4 | 141.7 | 141.9 |
| 5a′ | 146.7 | 146.5 | 144.1 |
| 8a′ | 117.0 | 116.1 | 117.4 |
| 3′-Me | 22.0 | 21.9 | 22.2 |
| 6′-OMe | 56.5 | 56.4 | 56.1 |
| 1″ | 106.2 | 106.3 | 105.1 |
| 2″ | 74.9 | 75.0 | 75.1 |
| 3″ | 78.8 | 78.7 | 78.5 |
| 4″ | 71.6 | 71.4 | 71.6 |
| 5″ | 77.5 | 77.5 | 76.8 |
| 6″ | 62.9 | 62.8 | 62.7 |
| 1′′′ | 104.9 | 104.5 | 105.0 |
| 2′′′ | 74.5 | 74.5 | 75.1 |
| 3′′′ | 78.8 | 78.6 | 78.4 |
| 4′′′ | 71.2 | 71.3 | 71.3 |
| 5′′′ | 77.4 | 77.5 | 76.8 |
| 6′′′ | 62.6 | 62.6 | 62.6 |
a 13C NMR data were measured in CD3OD at 150 MHz