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. 2017 Jul 5;41(6):617–624. doi: 10.1007/s12272-016-0816-7

Table 4.

13C NMR spectroscopic data of compounds 57

No. 5*a 6*a 7*a
1 162.2 162.2 161.9
2 117.4 117.5 117.5
3 146.7 146.8 147.7
4 121.9 121.9 121.2
5 113.0 110.9 113.3
6 166.1 165.4 164.1
7 108.1 107.8 106.3
8 162.0 161.8 161.7
9 188.4 188.6 188.6
10 57.3 57.6 57.3
1a 117.7 118.2 118.5
4a 139.8 140.6 141.9
5a 144.5 145.5 144.1
8a 116.5 117.8 116.1
3-Me 21.8 22.0 22.2
1′ 162.9 162.9 162.0
2′ 117.5 117.7 117.6
3′ 147.5 147.6 147.7
4′ 121.4 121.6 121.2
5′ 111.7 112.6 111.0
6′ 164.9 165.2 164.9
7′ 104.2 106.2 105.5
8′ 162.0 162.0 161.4
9′ 188.4 188.3 188.5
10′ 57.5 57.5 57.4
1a′ 117.9 117.2 118.6
4a′ 142.4 141.7 141.9
5a′ 146.7 146.5 144.1
8a′ 117.0 116.1 117.4
3′-Me 22.0 21.9 22.2
6′-OMe 56.5 56.4 56.1
1″ 106.2 106.3 105.1
2″ 74.9 75.0 75.1
3″ 78.8 78.7 78.5
4″ 71.6 71.4 71.6
5″ 77.5 77.5 76.8
6″ 62.9 62.8 62.7
1′′′ 104.9 104.5 105.0
2′′′ 74.5 74.5 75.1
3′′′ 78.8 78.6 78.4
4′′′ 71.2 71.3 71.3
5′′′ 77.4 77.5 76.8
6′′′ 62.6 62.6 62.6

a 13C NMR data were measured in CD3OD at 150 MHz