Table 3. Data collection and processing.
| Data set | VcNanE–GlcNAc-6-P | VcNanE | FnNanE |
|---|---|---|---|
| Diffraction source | PROXIMA-1, SOLEIL | PROXIMA-1, SOLEIL | PROXIMA-1, SOLEIL |
| Wavelength (Å) | 0.978 | 0.978 | 0.978 |
| Temperature (K) | 100 | 100 | 100 |
| Detector | Dectris PILATUS 6M | Dectris PILATUS 6M | Dectris PILATUS 6M |
| Crystal-to-detector distance (mm) | 346.9 | 384.9 | 441.3 |
| Rotation range per image (°) | 0.1 | 0.1 | 0.1 |
| Total rotation range (°) | 180 | 180 | 180 |
| Exposure time per image (s) | 0.1 | 0.1 | 0.1 |
| Space group | P212121 | P212121 | I222 |
| a, b, c (Å) | 48.96, 70.65, 149.36 | 49.32, 70.42, 150.40 | 47.52, 75.35, 135.88 |
| α, β, γ (°) | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 |
| Mosaicity (°) | 0.55 | 0.09 | 0.14 |
| Resolution range (Å) | 40.94–2.66 (2.75–2.66) | 46.87–1.70 (1.73–1.70) | 44.85–2.21 (2.27–2.21) |
| Total No. of reflections | 89562 (10022) | 365016 (13639) | 80920 (6997) |
| No. of unique reflections | 15416 (1900) | 58493 (2962) | 12687 (1086) |
| Multiplicity | 5.8 (5.3) | 6.2 (4.6) | 6.4 (6.4) |
| Completeness (%) | 99 (94.3) | 100 (100) | 100 (100) |
| Mean I/σ(I) | 8.7 (2.4) | 15.2 (3.7) | 13.5 (2.8) |
| Wilson B factor (Å2) | 43.5 | 17.8 | 49.6 |
| R meas | 0.152 (0.555) | 0.097 (0.473) | 0.076 (0.761) |
| R p.i.m. | 0.062 (0.230) | 0.038 (0.217) | 0.030 (0.297) |
| CC1/2 | 0.99 (0.92) | 0.99 (0.91) | 0.99 (0.78) |