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. 2018 Jun 13;25(Pt 4):1189–1195. doi: 10.1107/S1600577518006203

Table 2. Comparison of the lower limits of detection (LLD) for Ca, Fe and Cu determined for the B16 beamline at Diamond Light Source and the P06 beamline at PETRA III as well as some of the measurement parameters.

For both beamlines a multi-element standard was scanned to determine the LLDs for various elements. The values for the PETRA III P06 beamline are taken from Boesenberg et al. (2016).

  Diamond B16 PETRA III P06
Ca K LLD (in ag for 1000 s) 92 2.241
Fe K LLD (in ag for 1000 s) 13 0.226
Cu K LLD (in ag for 1000 s) 7 0.109
Standard NIST SRM 2783 AXO thin-film R11
Measurement time per pixel 120 s 20 ms
Excitation 12.7 keV 12 keV
Monochromator Multilayer Double-crystal monochromator
Spot size (vertical × horizontal) 500 nm × 600 nm 450 nm × 450 nm
Detector SDD Maia