| [Ni(NCS)2(C6H6N2S)4]·5CH4O | Z = 2 |
| Mr = 887.83 | F(000) = 928 |
| Triclinic, P1 | Dx = 1.392 Mg m−3 |
| a = 10.4520 (3) Å | Mo Kα radiation, λ = 0.71073 Å |
| b = 14.5934 (4) Å | Cell parameters from 30865 reflections |
| c = 15.0580 (5) Å | θ = 1.5–27.0° |
| α = 101.553 (2)° | µ = 0.80 mm−1 |
| β = 97.105 (2)° | T = 200 K |
| γ = 106.417 (2)° | Block, yellow |
| V = 2118.43 (11) Å3 | 0.30 × 0.18 × 0.10 mm |