Table 4. Hydrogen-bond geometry (Å, °) for 2 .
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O1—H1⋯S2i | 0.84 | 2.88 | 3.409 (2) | 123 |
| O1—H1⋯S11ii | 0.84 | 2.92 | 3.578 (2) | 137 |
| O2—H2⋯S31iii | 0.84 | 2.62 | 3.413 (3) | 157 |
| O3—H3⋯S1iv | 0.84 | 2.77 | 3.427 (2) | 136 |
| O3—H3⋯S31v | 0.84 | 2.93 | 3.576 (2) | 135 |
| C5—H5A⋯S31v | 0.98 | 3.03 | 3.632 (4) | 121 |
| O4—H4⋯O5 | 0.84 | 1.92 | 2.708 (5) | 156 |
| C6—H6B⋯S31vi | 0.98 | 2.73 | 3.566 (4) | 143 |
| O5—H5⋯S41vii | 0.84 | 2.51 | 3.216 (3) | 142 |
| C7—H7A⋯S41vii | 0.98 | 2.93 | 3.528 (5) | 121 |
| C11—H11⋯N1 | 0.95 | 2.52 | 3.063 (3) | 117 |
| C11—H11⋯S1viii | 0.95 | 2.73 | 3.442 (2) | 133 |
| C12—H12⋯S1viii | 0.95 | 2.96 | 3.542 (2) | 121 |
| C15—H15⋯N2 | 0.95 | 2.61 | 3.097 (3) | 113 |
| N12—H1N⋯O2 | 0.88 | 2.02 | 2.898 (3) | 177 |
| N12—H2N⋯S2ix | 0.88 | 2.58 | 3.446 (2) | 171 |
| C21—H21⋯N1 | 0.95 | 2.65 | 3.109 (3) | 110 |
| C25—H25⋯N2 | 0.95 | 2.66 | 3.122 (3) | 111 |
| C25—H25⋯S2x | 0.95 | 2.94 | 3.846 (2) | 159 |
| N22—H4N⋯S2xi | 0.88 | 2.64 | 3.4939 (19) | 163 |
| N22—H3N⋯O1 | 0.88 | 2.10 | 2.978 (3) | 174 |
| N32—H5N⋯O5 | 0.88 | 1.95 | 2.833 (3) | 180 |
| N32—H6N⋯S1vi | 0.88 | 2.64 | 3.478 (2) | 159 |
| C45—H45⋯S11ix | 0.95 | 2.89 | 3.673 (2) | 141 |
| N42—H7N⋯O3 | 0.88 | 2.08 | 2.957 (3) | 173 |
| N42—H8N⋯S1xii | 0.88 | 2.88 | 3.749 (2) | 169 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
; (ix)
; (x)
; (xi)
; (xii)
.