Table 4. Experimental details.
| Crystal data | |
| Chemical formula | C20H13NO2S2 |
| M r | 363.43 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 298 |
| a, b, c (Å) | 7.6461 (8), 9.8772 (9), 11.2191 (12) |
| α, β, γ (°) | 72.571 (5), 88.496 (6), 86.144 (6) |
| V (Å3) | 806.54 (14) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.34 |
| Crystal size (mm) | 0.25 × 0.20 × 0.20 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2012 ▸) |
| T min, T max | 0.921, 0.934 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 16616, 3174, 2458 |
| R int | 0.036 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.034, 0.091, 1.03 |
| No. of reflections | 3102 |
| No. of parameters | 226 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.24, −0.41 |