Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H14IN3O2·CH4O |
| M r | 427.23 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 12.9877 (10), 14.8982 (10), 8.5593 (6) |
| β (°) | 91.806 (2) |
| V (Å3) | 1655.3 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.95 |
| Crystal size (mm) | 0.41 × 0.27 × 0.22 |
| Data collection | |
| Diffractometer | Bruker D8 Quest CMOS |
| Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
| T min, T max | 0.613, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 45415, 3394, 3086 |
| R int | 0.044 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.017, 0.041, 1.06 |
| No. of reflections | 3394 |
| No. of parameters | 231 |
| No. of restraints | 1 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.61, −0.24 |